HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Toluidine → HCID 86734245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Toluidine | HCID 7934 | — |
| Reactant | HCID 86734246 | HCID 86734246 | — |
| Reactant | N,N-dimethyl-N-(3-amino-4-methoxybenzyl)-N-3-aminopropylammonium chloride | HCID 86734247 | — |
| Product | HCID 86734245 | HCID 86734245 | — |
Reaction Steps
Proceeding in a manner similar to that described above in Example 3, N,N-dimethyl-N-(3-amino-4-methoxybenzyl)-N-3-formamidopropylammonium chloride was hydrolzed and the resulting N,N-dimethyl-N-(3-amino-4-methoxybenzyl)-N-3-aminopropylammonium chloride was diazotized and coupled with meta-toluidine to obtain N,N-dimethyl-N-[3-(4-amino-2-methylphenyl)azo-4-methoxybenzyl]-N-3-aminopropylammonium chloride in aqueous solution. This product was diazotized in situ and coupled with 4'-chloroacetoacetanilide to obtain the yellow, water-soluble dyestuff having the formula ##STR137##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04103092 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-398870b223e444579c5c3583d90951ef |
| Source note | uspto-grants-1978_07 |