HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butynedioic acid → HCID 54401087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butynedioic acid | HCID 371 | — |
| Reactant | 1-(3,4-dichlorophenyl)-3-methylthiourea | HCID 2808839 | — |
| Product | HCID 54401087 | HCID 54401087 | 64.7% |
Reaction Steps
Prepared by the method described in Example 1 from N-methyl-N'-(3,4-dichlorophenyl)thiourea (4.9 g, 21 mmoles) and acetylenedicarboxylic acid (2.6 g, 22 mmoles). Recrystallization from ethyl acetate gave the product (4.5 g), mp 225°-226° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04775677 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-6fe99a330e724cf9b9e2ab646af7dd15 |
| Source note | uspto-grants-1988_10 |