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HRID867439

反应详情

EQUATION

反应方程式

HRID 867439 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C#CC(=O)O
HCID371

2-Butynedioic acid

C4H2O4

结构：CCCCCCNC(=S)Nc1ccccc1
HCID2759282

1-Hexyl-3-phenyl-2-thiourea

C13H20N2S

PRODUCTS

生成物

1
结构：CCCCCCN1C(=O)C(=CC(=O)O)SC1=Nc1ccccc1
HCID54073641

未命名化合物

收率 64.5%

PROCEDURE

实验过程

Prepared by the method described in Example 1 from N-hexyl-N'-phenylthiourea (3.4 g, 14 mmoles) and acetylenedicarboxylic acid (1.7 g, 14 mmoles). Recrystallization from acetonitrile gave the product (3.0 g), mp 145°-146° C.

WORKUP

后处理

  1. customPrepared by the method
  2. customRecrystallization from acetonitrile