HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butynedioic acid → HCID 54267842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butynedioic acid | HCID 371 | — |
| Reactant | HCID 14390156 | HCID 14390156 | — |
| Product | HCID 54267842 | HCID 54267842 | 13.1% |
Reaction Steps
Prepared by the method described in Example 21 from N,N'-bis(3,4-dibromophenyl)thiourea (13.7 g, 25 mmoles) and acetylenedicarboxylic acid (2.7 g, 25 mmoles). Recrystallization from methanol gave the product (2.1 g), mp 235°-237° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04775677 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-8bcfc56e3664409a9192b7768e5b4949 |
| Source note | uspto-grants-1988_10 |