Iodine → HCID 14281035, compound

HRID 867500Notes

Reaction equation

HRID 867500 reaction equation
II.[C:3]([O:6][CH2:7][CH2:8][O:9][C:10]1[CH:15]=[CH:14][C:13]([N+:16]([O-])=O)=[C:12]([CH:19]=[C:20]2[NH:24][C:23](=[O:25])[NH:22][C:21]2=O)[CH:11]=1)(=[O:5])[CH3:4]>C(#N)C>[C:3]([O:6][CH2:7][CH2:8][O:9][C:10]1[CH:15]=[CH:14][C:13]2[N:16]=[C:21]3[NH:22][C:23](=[O:25])[NH:24][C:20]3=[CH:19][C:12]=2[CH:11]=1)(=[O:5])[CH3:4]

Participants

4

Reactant 2

HCID 807IodineHCID 70414395HCID 70414395, compound

Product 1

HCID 14281035HCID 14281035, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

This compound, m.p. 299°-302° C. (dec.), was prepared analogous to Example 10 (using acetonitrile in place of methanol for the iodine treatment) from 2-[3-[(2,4-dioxoimidazolidin-5-ylidene)methyl]-4-nitrophenoxy]ethyl acetate.

Workup

  1. customThis compound, m.p. 299°-302° C. (dec.), was prepared analogous to Example 10 (

Sources & evidence

ORD record
ord-8ca05c21d06c491a8e346a8576b8c221
Source dataset
uspto-grants-1988_10
Patent number
US04775674

Reaction notes

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