HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → Allyl methacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| Reactant | Butyl Methacrylate | HCID 7354 | — |
| Reactant | HCID 178435178 | HCID 178435178 | — |
| Solvent | Water | HCID 962 | — |
| Product | Allyl methacrylate | HCID 7274 | — |
| Product | Butyl Methacrylate | HCID 7354 | — |
Reaction Steps
A trimer of butyl methacrylate and allyl methacrylate, which was prepared analogously to the dimer in Example 1, was added to the mixture containing 90 wt.-% N-vinylpyrrolidone and 10 wt.-% butyl methacrylate in the amount of 1 wt.-% on the whole mixture. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 72 wt.-% water at G=0.023 MPa.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04775731 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-18210995d7a3465bb96dd0abd22accc3 |
| Source note | uspto-grants-1988_10 |