Nicotinic Acid → HCID 531640, compound

HRID 867618Notes

Reaction equation

HRID 867618 reaction equation
[CH2:1]([OH:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].[C:15](O)(=[O:22])[C:16]1[CH:21]=[CH:20][CH:19]=[N:18][CH:17]=1>>[C:15]([O:14][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13])(=[O:22])[C:16]1[CH:21]=[CH:20][CH:19]=[N:18][CH:17]=1

Participants

3

Reactant 2

HCID 938Nicotinic AcidHCID 82071-Tridecanol

Product 1

HCID 531640HCID 531640, compound

Procedure

Tridecyl nicotinate was prepared using the method of Example 1 from commercial tridecanol (an isomeric mixture) and nicotinic acid. The product had a boiling point of 136° to 140° C. under 0.05 mm pressure and an estimated purity of 100% based on a molecular weight of 305.5.

Sources & evidence

ORD record
ord-803bfdbfc07344ca9076a4b28dec07a4
Source dataset
uspto-grants-1988_10
Patent number
US04775763

Reaction notes

Loading…