HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Azido-2,3,5,6-tetrachloropyridine → 2-Azido-6-chloropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Azido-2,3,5,6-tetrachloropyridine | HCID 6425094 | — |
| Reactant | 2-Azido-6-(trifluoromethyl)pyridine | HCID 13339347 | — |
| Reactant | 2-Azido-6-bromopyridine | HCID 21290342 | — |
| Reactant | 2-Azido-6-fluoropyridine | HCID 21290353 | — |
| Reactant | 3-Azido-5-(trifluoromethyl)pyridine | HCID 21290356 | — |
| Product | 2-Azido-6-chloropyridine | HCID 21576379 | — |
Reaction Steps
The following were prepared analogously and analyzed by nmr spectroscopy: 2-azido-6-bromopyridine, m.p. 106°-110° C.; 2-azido-6-fluoropyridine, m.p. 45°-48° C.; 2-azido-6-(trifluoromethyl)pyridine, brown oil; 3-azido-5-(trifluoromethyl)pyridine, dark oil; 4-azido-2,3,5,6-tetrachloropyridine, light brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04775762 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-3690cff768944c5587850cba2a072ad1 |
| Source note | uspto-grants-1988_10 |