HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 178480237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 4-(2-Fluorobenzoyl)-1-methylpiperidine | HCID 13180317 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178480237 | HCID 178480237 | 23.7% |
Reaction Steps
An autoclave was charged with 10.0 g of 4-(2-fluorobenzoyl)-1-methylpiperidine and 14 ml of hydrazine hydrate. The reaction was heated at 150° for 20 hrs, cooled, and poured into water. The resultant solid was collected. The solid was recrystallized twice from toluene to yield 2.4 g (23.7%) of product, mp 168°-170° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04775761 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-03931d858f4e46539cd9a9bd28f5b765 |
| Source note | uspto-grants-1988_10 |