HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178524324, compound → HCID 88615862, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178524324 | HCID 178524324 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 88615862 | HCID 88615862 | — |
Reaction Steps
8.5 g (0.029 mol) 6-benzylthiopyridine-2,3-dicarboxylic acid are stirred into 150 ml acetanhydride 6 hours at 110° C. The substrate thereby dissolves completely. The solvent is distilled off in a vacuum and the residue is employed in the next stage without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04776876 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-c3499dadab6d47deaf546e2f7eabe3c1 |
| Source note | uspto-grants-1988_10 |