Tetramethylammonium Methyl Carbonate → Methanaminium, N,N,N-trimethyl-, carbonate (1:1)

HRID 867847Notes

Reaction equation

HRID 867847 reaction equation
C[O:2][C:3](=[O:5])[O-:4].[CH3:6][N+:7]([CH3:10])([CH3:9])[CH3:8]>O>[C:3](=[O:2])([O-:5])[OH:4].[CH3:6][N+:7]([CH3:10])([CH3:9])[CH3:8]

Participants

3

Reactant 1

HCID 11804927Tetramethylammonium Methyl Carbonate

Product 1

HCID 10197721Methanaminium, N,N,N-trimethyl-, carbonate (1:1)

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

108.0 g of tetramethylammonium monomethylcarbonate and 72.0 g of water were introduced in the same reactor as used in Preparation Example 1 and heated with stirring. After the temperature in the reactor reached 100° C., the reaction was continued for 3 hours at 100° C. Tetramethylammonium hydrogencarbonate was obtained in a yield of 96.7 mol %.

Workup

  1. customas used in Preparation Example 1
  2. temperatureheated
  3. customreached 100° C.

Sources & evidence

ORD record
ord-bb5d211d99a745358aa0b2b9aa21c661
Source dataset
uspto-grants-1988_10
Patent number
US04776929

Reaction notes

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