HCID 19871551, compound → HCID 85570074, compound

HRID 867850Notes

Reaction equation

HRID 867850 reaction equation
C[O:2][C:3](=[O:5])[O-:4].[CH3:6][N+:7]([CH3:11])([CH3:10])[CH2:8][CH3:9]>O>[C:3](=[O:2])([O-:5])[OH:4].[CH3:6][N+:7]([CH3:11])([CH3:10])[CH2:8][CH3:9]

Participants

3

Reactant 1

HCID 19871551HCID 19871551, compound

Product 1

HCID 85570074HCID 85570074, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

114.1 g of trimethylethylammonium monomethylcarbonate and 75.6 g of water were introduced in the same reactor as used in Preparation Example 1 and heated with stirring. After the temperature in the reactor reached 120° C., the reaction was continued for 3 hours at 120° C. Trimethylethylammonium hydrogencarbonate was obtained in a yield of 96.3 mol %.

Workup

  1. customas used in Preparation Example 1
  2. temperatureheated
  3. customreached 120° C.

Sources & evidence

ORD record
ord-13ae56ff8ff94768903a653a32d808d9
Source dataset
uspto-grants-1988_10
Patent number
US04776929

Reaction notes

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