HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 13712845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 6-Methoxychromone | HCID 688880 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13712845 | HCID 13712845 | — |
Reaction Steps
A solution of 6-methoxy-4-benzopyranone (31.6 g), triethylamine (4.9 ml) and 10% palladium on carbon (3.16 g) in absolute ethanol (1.7 l) is stirred under an atmosphere of hydrogen for 19 hours. The reaction mixture is filtered and evaporated in vacuo yielding the desired hydrogenated product as a pale yellow liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04777168 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-b09f7850e1d8464c912ce97e8a11c136 |
| Source note | uspto-grants-1988_10 |