HCID 19967810, compound → HCID 19819012, compound

HRID 867900Notes

Reaction equation

HRID 867900 reaction equation
[C:1]([N:4]1[C:8]2=[C:9]([Cl:16])[C:10]([C:12]([CH3:15])([CH3:14])[CH3:13])=[N:11][N:7]2[C:6]([C:17]2[C:22]([CH3:23])=[CH:21][C:20]([CH3:24])=[C:19]([N+:25]([O-])=O)[C:18]=2[CH3:28])=[N:5]1)(=[O:3])[CH3:2].C(N1C2=CC(C(C)(C)C)=NN2C(C2C(C)=CC(C)=C(N)C=2C)=N1)(=O)C>>[C:1]([N:4]1[C:8]2=[C:9]([Cl:16])[C:10]([C:12]([CH3:15])([CH3:14])[CH3:13])=[N:11][N:7]2[C:6]([C:17]2[C:22]([CH3:23])=[CH:21][C:20]([CH3:24])=[C:19]([NH2:25])[C:18]=2[CH3:28])=[N:5]1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 19967810HCID 19967810, compoundHCID 21288864HCID 21288864, compound

Product 1

HCID 19819012HCID 19819012, compound

Procedure

The product of part (a) of this Example (24.3 g, 60.1 mmole) was reduced under the conditions described in part (b) of Example 6 to give after chromatography the partially hydrated product in p. 211°-213° C., 15.5 g (77%).

Workup

  1. customto give after chromatography the partially hydrated product in p
  2. custom211°-213° C., 15.5 g (77%)

Sources & evidence

ORD record
ord-dfd1bf3fdc9e4124a741bbc2827b137c
Source dataset
uspto-grants-1988_10
Patent number
US04777121

Reaction notes

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