HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 86742470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 6-Carbamimidoylnaphthalen-2-yl methanesulfonate | HCID 13050560 | — |
| Reactant | HCID 67935692 | HCID 67935692 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 86742470 | HCID 86742470 | 63.6% |
Reaction Steps
Alternatively, 4 g of 4-(2-imidazolinyl)amino-benzoic acid hydrochloride, 4.67 g of 6-amidino-2-naphthol methanesulfonate and 0.2 g of DMAP were dissolved in 60 ml of anhydrous pyridine, 5.13 g of DCC was added to the solution and then the reaction mixture was treated as described above, via a carbonate salt, to yield 2.35 g of 6-amidino-2-naphthyl 4-(2-imidazolinyl)amino-benzoate dihydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04777182 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-9ec3baf67f1e449990ef2d3226cdc8f4 |
| Source note | uspto-grants-1988_10 |