HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → 3-[3-(2-Azepan-1-yl-ethoxy)-phenyl]-thieno[2,3-d]isoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-[3-(2-Bromo-ethoxy)-phenyl]-thieno[2,3-d]isoxazole | HCID 21983582 | — |
| Product | 3-[3-(2-Azepan-1-yl-ethoxy)-phenyl]-thieno[2,3-d]isoxazole | HCID 9798141 | — |
Reaction Steps
The title compound is prepared from 3-[3-(2-bromo-ethoxy)-phenyl]-thieno[2,3-d]isoxazole, potassium carbonate, hexamethyleneimine and acetonitrile essentially as described above in example 40. Purity by LC/MS (APCI)=99%, [M+H]+=343.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07091199B1 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-6c2c563a30e04c3f95fd9e00eaaedf6d |
| Source note | uspto-grants-2006_08 |