HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-diethyl-1-(phenylmethyl)-3-pyrrolidinemethanamine → N,N-Diethyl-3-pyrrolidinemethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-diethyl-1-(phenylmethyl)-3-pyrrolidinemethanamine | HCID 14075472 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N,N-Diethyl-3-pyrrolidinemethanamine | HCID 14075474 | 101.7% |
Reaction Steps
A mixture of 25.4 g (0.10 mole) of N,N-diethyl-1-(phenylmethyl)-3-pyrrolidinemethanamine, 200 ml of methyl alcohol, 2 g of palladium on carbon and hydrogen were shaken at a pressure of 51.5 psi. After 20.3 hours, the catalyst was filtered and the filtrate concentrated under reduced pressure. The residue was bulb to bulb distilled giving 15.9 g of N,N-diethyl-3-pyrrolidinemethanamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04777175 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-ba76fa491f504560a6f9994f141446a8 |
| Source note | uspto-grants-1988_10 |