HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 14307644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 14307643 | HCID 14307643 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14307644 | HCID 14307644 | — |
Reaction Steps
To a solution of the product of Example 11 (247 mg, 0.66 mmol) in CH2Cl2 (30 mL) was added m-chloroperbenzoic acid (140 mg). The reaction was complete in a few minutes, and was quenched with 10% NaCO3. The organic layer was separated, dried (Na2SO4) and the crude product was chromatographed on silica gel (30% EtOAc/hexane) to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04778805 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-bf7f6d2ee5364dc9bcd62d658b096893 |
| Source note | uspto-grants-1988_10 |