HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroquinone → Butyl (acryloylamino)(butoxy)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Dimethyl Ether | HCID 8254 | — |
| Reactant | Acetic acid, 2-hydroxy-2-[(1-oxo-2-propen-1-yl)amino]- | HCID 92230 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Butyl (acryloylamino)(butoxy)acetate | HCID 57312822 | — |
Reaction Steps
One hundred parts of acrylamidoglycolic acid (AGA); 517 parts butanol, 1 part concentrated sulfuric acid and 0.1 part monomethyl ether of hydroquinone were mixed in a flask equipped with a Dean Stark water trap and a stirrer. The mixture was heated until homogeneous. After 5-10 minutes 100 ml of toluene was added and the mixture was brought to reflux and held 5 hours until the theoretical amount of water was collected by azeotrope.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04778869 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-11d9c9df65bf47f8965db450752fdb1c |
| Source note | uspto-grants-1988_10 |