Epibromohydrin → HCID 15078344, compound

HRID 868381Notes

Reaction equation

[OH:1][C:2]1[CH:18]=[CH:17][C:5]2[CH2:6][CH2:7][CH:8]([CH2:10][CH2:11][C:12]([O:14][CH2:15][CH3:16])=[O:13])[O:9][C:4]=2[C:3]=1[CH2:19][CH2:20][CH3:21].[CH2:22]([CH:24]1[O:26][CH2:25]1)Br>>[O:26]1[CH2:25][CH:24]1[CH2:22][O:1][C:2]1[CH:18]=[CH:17][C:5]2[CH2:6][CH2:7][CH:8]([CH2:10][CH2:11][C:12]([O:14][CH2:15][CH3:16])=[O:13])[O:9][C:4]=2[C:3]=1[CH2:19][CH2:20][CH3:21]

Participants

Reactant 2

HCID 18430Epibromohydrin

HCID 14882995HCID 14882995, compound

Product 1

HCID 15078344HCID 15078344, compound

Procedure

The title compound was prepared by the method of Example 11 using 3.0 g (10.3 mmole) of the product of Example 27 and 1.3 ml (15 mmole) of epibromohydrin as starting materials. Structure assignment was supported by nmr and infrared spectra.

Sources & evidence

ORD record: ord-ba858460690044ca822ad3f17ffd4ae7
Source dataset: uspto-grants-1988_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04778903

Reaction notes

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