HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70350594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 70350596 | HCID 70350596 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70350594 | HCID 70350594 | — |
Reaction Steps
A solution of benzyl-3-(hexanoyl)phenyl ether (2.8 g.), 40% aqueous methylamine (1.5 ml) and methanol adjusted to pH 6 with 5% aqueous hydrochloric acid is treated with a methanolic solution of sodium cyanoborohydride. The reaction is stirred overnight. The methanol is removed in vacuo and the remaining mixture is extracted with methylene chloride. The organic extract is dried (MgSO4) and concentrated to an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04778931 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-ef19ccc812bc419cbb149565724231b3 |
| Source note | uspto-grants-1988_10 |