HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 4-(2-Nonyloxyphenyl)-3-butene-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 13785718 | HCID 13785718 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Sodium chloride; water | HCID 57417360 | — |
| Product | 4-(2-Nonyloxyphenyl)-3-butene-2-one | HCID 54077108 | — |
Reaction Steps
2-(nonyloxy)benzaldehyde (62 g) dissolved in acetone (500 mL) was treated with aqueous sodium hydroxide (100 mL, 1M) at room temperature for 18 h. Brine and ethyl acetate/hexane (1:1 parts by volume) was then added. Concentration of the organic phase followed by crystallization from hexane gave 4-(2-nonyloxyphenyl)-3-butene-2-one (53 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780251 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-4dac9e35efda490286c505b9585514ee |
| Source note | uspto-grants-1988_10 |