化工社化工社 化学情報印刷レポート · 研究参考用
Cyclopentylamine → N-cyclopentyl-1-propyl[1,2,4]triazolo[4,3-a]quinoxalin-4-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclopentylamine | HCID 2906 | — |
| 反応物 | 4-Chloro-1-propyl[1,2,4]triazolo[4,3-a]quinoxaline | HCID 13385707 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | N-cyclopentyl-1-propyl[1,2,4]triazolo[4,3-a]quinoxalin-4-amine | HCID 14280611 | 82.9% |
反応手順
A reaction mixture of 4-chloro-1-propyl[1,2,4]triazolo[4,3-a]quinoxaline (1.0 g; 0.004 mole) and cyclopentanamine (1.0 g; 0.012 mole) in 15 ml of DMF was stirred at room temperature for 20 hours. The precipitated solid was filtered, washed with ethanol, and dried affording 0.98 g (82%) of N-cyclopentyl-1-propyl[1,2,4]triazolo[4,3-a]quinoxalin-4-amine having a mp of 186°-188° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04780464 |
| 出典データセット | uspto-grants-1988_10 |
| ORD ID | ord-f2ad039bb3c44e1e802c1daac48e2ee6 |
| 出典メモ | uspto-grants-1988_10 |