huagongshe.com
HRID868587

反应详情

EQUATION

反应方程式

HRID 868587 的结构方程式

REACTANTS

反应物

2
结构：Cl.NNC(N)=O
HCID11236

Semicarbazide hydrochloride

CH6ClN3O

结构：CC(C)N(CCCN1C(=O)C(=O)c2ccccc21)C(C)C
HCID13934420

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)N(CCCN1C(=O)/C(=N/NC(N)=O)c2ccccc21)C(C)C
HCID178457307

未命名化合物

收率 66.6%

PROCEDURE

实验过程

By using 1-(3-diisopropylaminopropyl)isatin and semicarbazide hydrochloride, a method analogous to that described in Example 4 was carried out to obtain (E)-1-(3-diisopropylaminopropyl)isatin 3-semicarbazone having a melting point of 173°-175° C. (yield: 66.6%, recrystallizing solvent: methanol-benzene).