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HRID868597

反应详情

EQUATION

反应方程式

HRID 868597 的结构方程式

REACTANTS

反应物

2
结构：Cl.NNC(N)=O
HCID11236

Semicarbazide hydrochloride

CH6ClN3O

结构：CC(C)N(CCN1C(=O)C(=O)c2cc(Br)ccc21)C(C)C
HCID13934415

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)N(CCN1C(=O)/C(=N/NC(N)=O)c2cc(Br)ccc21)C(C)C
HCID178457373

未命名化合物

收率 72.6%

PROCEDURE

实验过程

By using 5-bromo-1-(2-diisopropylaminoethyl)isatin and semicarbazide hydrochloride, a method analogous to that described in Example 4 was carried out to obtain (E)-5-bromo-1-(2-diisopropylaminoethyl)isatin 3-semicarbazone having a melting point of 149°-153° C. (yield: 72.6%, recrystallizing solvent: chloroform-hexane).