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HRID868598

反应详情

EQUATION

反应方程式

HRID 868598 的结构方程式

REACTANTS

反应物

2
结构：NNC(=O)NC1CCCCC1
HCID261879

n-cyclohexylhydrazinecarboxamide

C7H15N3O

结构：CC(C)N(CCN1C(=O)C(=O)c2cc(Br)ccc21)C(C)C
HCID13934415

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)N(CCN1C(=O)/C(=N/NC(=O)NC2CCCCC2)c2cc(Br)ccc21)C(C)C
HCID178457391

未命名化合物

收率 89.9%

PROCEDURE

实验过程

By using 5-bromo-1-(2-diisopropylaminoethyl)isatin and 4-cyclohexylsemicarbazide, a method analogous to that described in Example 16 was carried out to obtain (E)-5-bromo-1-(2-diisopropylaminoethyl)isatin 3-(4-cyclohexylsemicarbazone) having a melting point of 155°-156° C. (yield: 89.9%, recrystallizing solvent: chloroform-hexane).