HuagongsheHuagongshe Chemistry Print Report · For research reference only
Semicarbazide hydrochloride → HCID 178487249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Semicarbazide hydrochloride | HCID 11236 | — |
| Reactant | HCID 13934417 | HCID 13934417 | — |
| Product | HCID 178487249 | HCID 178487249 | 84% |
Reaction Steps
By using 1-(2-diisopropylaminoethyl)-5-methoxyisatin and semicarbazide hydrochloride, a method analogous to that described in Example 6 was carried out to obtain (E)-1-(2-diisopropylaminoethyl)-5-methoxyisatin 3-semicarbazone having a melting point of 157°-159° C. (yield: 84.0%, recrystallizing solvent: ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780477 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-043687bdb71c468ba549cad6ae30c09e |
| Source note | uspto-grants-1988_10 |