HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Benzothiophene 1,1-dioxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Benzo(B)Thiophene | HCID 7221 | — |
| Product | Benzothiophene 1,1-dioxide | HCID 69997 | — |
Reaction Steps
A solution of 40 grams of thianaphthene (Aldrich Chemical Co.), acetic acid (240 ml) and 30% hydrogen peroxide (180 ml) was heated at reflux for 15 minutes. This solution was added to water (800 ml), cooled and filtered to give thianaphthene-1,1-dioxide, m.p.--142°-143° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780480 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-771635f94d434e7dbd7ec22af284e105 |
| Source note | uspto-grants-1988_10 |