Isopropylamine → HCID 21268557, compound

HRID 868631Notes

Reaction equation

HRID 868631 reaction equation
[CH3:1][C:2]1[CH:22]=[CH:21][C:5]([C:6]([C:8]2[C:16]3[O:15][CH:14]=[CH:13][C:12]=3[CH:11]=[C:10]([CH2:17][C:18]([OH:20])=[O:19])[CH:9]=2)=[S:7])=[CH:4][CH:3]=1.[CH:23]([NH2:26])([CH3:25])[CH3:24]>C1C=CC=CC=1>[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([C:6]([C:8]2[C:16]3[O:15][CH:14]=[CH:13][C:12]=3[CH:11]=[C:10]([CH2:17][C:18]([OH:20])=[O:19])[CH:9]=2)=[S:7])=[CH:21][CH:22]=1.[CH:23]([NH2:26])([CH3:25])[CH3:24].[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([C:6]([C:8]2[C:16]3[O:15][CH:14]=[CH:13][C:12]=3[CH:11]=[C:10]([CH2:17][C:18]([OH:20])=[O:19])[CH:9]=2)=[S:7])=[CH:21][CH:22]=1

Participants

5

Reactant 2

HCID 6363IsopropylamineHCID 21268557HCID 21268557, compound

Product 2

HCID 21268557HCID 21268557, compoundHCID 21287552HCID 21287552, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

A solution of 200 mg of (7-(4-methylthiobenzoyl)benzofuran-5-ylacetic acid in 15 ml of hot benzene is treated with 60 mg of isopropylamine. The solution is allowed to cool to room temperature and the product filtered off, washed with ether and dried to yield the isopropylamine salt of 7-(4-methylthiobenzoyl)benzofuran-5-ylacetic acid.

Workup

  1. filtrationthe product filtered off
  2. washwashed with ether
  3. customdried

Sources & evidence

ORD record
ord-d4208766218d4908b12c21b9366cf0e9
Source dataset
uspto-grants-1988_10
Patent number
US04780480

Reaction notes

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