HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 868767Generated: October 31, 2026
Triethyl phosphite → HCID 13409682, compound
https://huagongshe.com/reaction/868767
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | Phenanthrene, 9-(bromomethyl)- | HCID 185571 | — |
| Product | HCID 13409682 | HCID 13409682 | 56.8% |
Reaction Steps
9-(Bromomethyl)phenanthrene (18 g, 66.4 mmol) and triethyl phosphite (10.7 g) were mixed and heated to 150° C. under N2 for 4 h. The reaction mixture was concentrated and the residue was purified by silica gel column chromatography to yield 12 g of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08968887B2 |
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| Source dataset | uspto-grants-2015_03 |
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| ORD ID | ord-e1bd103fb28843de9fc00718c9d778bc |
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| Source note | uspto-grants-2015_03 |
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