HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthaleneacetic acid → HCID 131732521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthaleneacetic acid | HCID 11393 | — |
| Reactant | Ethyl bromophenylacetate | HCID 97780 | — |
| Reactant | Hydrazinium chloride | HCID 115031 | — |
| Product | HCID 131732521 | HCID 131732521 | — |
Reaction Steps
This is made in a analogous fashion to example 11 starting with 2-Naphthyl acetic acid, ring expansion with hydrazine hydrochloride, alkylation with Ethyl-alpha-bromophenylacetate, and saponification to give the title compound. 16.4% overall yield, LC/MS (M++1): 421.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969348B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-6e1c6a30696349fda7a83a38651df6d4 |
| Source note | uspto-grants-2015_03 |