HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 89601811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Potassium bis(trimethylsilyl)amide | HCID 3251421 | — |
| Reactant | HCID 89601326 | HCID 89601326 | — |
| Product | HCID 89601811 | HCID 89601811 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described for example 74 but using the compound prepared in example 88, 1 equivalent of KHMDS and 5 equivalents of ethyl chloroformate. No purification was performed. tR: 1.42 min (LC-MS 1); ESI-MS: 582.2 [M+H]+ (LC-MS 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969341B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-ec703f722b3249389aa2da4587fe316a |
| Source note | uspto-grants-2015_03 |