HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 11650157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 11527387 | HCID 11527387 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 11650157 | HCID 11650157 | — |
Reaction Steps
The compound obtained in Example 2-19 (0.165 g) and lithium hydroxide (45 mg) were added to tetrahydrofuran (4 ml) and water (2 ml). The same manner to Example 2-12 was conducted to give the titled compound as a white solid. Yield: 80 mg (51%); mp 175-176° C., MS APC-ve 604 (M−H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969362B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-ab53946f9682476fa1e7404b51a4445d |
| Source note | uspto-grants-2015_03 |