反应详情

Methyl (3-aminophenyl)acetate (1 g) and 1,2-dibromoethane (5 ml) were heated at 100° C. for 5 hours. After cooling, the resultant was purified by column chromatography (ethyl acetate:isohexane 7:3) to give the titled compound as an oil. Yield: 280 mg (17%).

1. temperatureAfter cooling
2. customthe resultant was purified by column chromatography (ethyl acetate:isohexane 7:3)