HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 869418Generated: October 30, 2026
HCID 86722263, compound → HCID 178488263, compound
https://huagongshe.com/reaction/869418
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 86722263 | HCID 86722263 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178488263 | HCID 178488263 | 65.8% |
Reaction Steps
A mixture of 16B (1.1 g, 2.3 mmol) and MnO2 (6 g) in THF (20 mL) was heated to 110° C. and reacted overnight. TLC monitored the reaction. After the reaction completed, the reaction mixture was filtered and the filtrate was concentrated to give 16C (0.7 g, 63.9% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08969373B2 |
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| Source dataset | uspto-grants-2015_03 |
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| ORD ID | ord-5528cf74dfc54dfeac025641fb32599e |
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| Source note | uspto-grants-2015_03 |
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