HRID869504

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID242950

2-(methoxymethyl)-1H-benzimidazole

C9H10N2O

结构：C/C(C#N)=C1/c2ccc(CBr)cc2COc2cc(F)ccc21

HCID86721333

未命名化合物

PRODUCTS

生成物

$结构：COCc1nc2ccccc2n1Cc1ccc2c(c1)COc1cc(F)ccc1/C2=C(\C)C#N$

HCID86721332

未命名化合物

收率 87%

PROCEDURE

实验过程

Using 2-methoxymethyl-1H-benzo[d]imidazole (Journal of Organometallic Chemistry, 2008, vol. 26, p 3889; 244 mg, 1.51 mmol) and (E)-2-[8-(bromomethyl)-3-fluorodibenzo[b,e]oxepin-11(6H)-ylidene]propanenitrile (550 mg, 1.54 mmol) obtained in Reference Example 1, and in the same manner as in Reference Example 1A, the title compound (576 mg, 87%) was obtained.

WORKUP

后处理

customobtained in Reference Example 1