HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butoxycarbonylalanine → methyl N-(tert-butoxycarbonyl)-L-alanyl-L-threoninate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butoxycarbonylalanine | HCID 85082 | — |
| Reactant | Ethyl L-threoninate hydrochloride | HCID 2763096 | — |
| Product | methyl N-(tert-butoxycarbonyl)-L-alanyl-L-threoninate | HCID 11483528 | — |
Reaction Steps
The preparation was performed in a similar manner as Example 1.001 (d) Method B from N-(tert-butoxycarbonyl)-L-alanine (5.62 g, 29.7 mmol) and L-threonine ethyl ester hydrochloride (4.58 g, 27.0 mmol) to give methyl N-(tert-butoxycarbonyl)-L-alanyl-L-threoninate. MS (APCI): m/z 305 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969376B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-27ce3ecf8b2f4529b00fc465cc54cbe3 |
| Source note | uspto-grants-2015_03 |