HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → (E)-3-(1-phenylmethanesulfonyl-1H-pyrrol-3-yl)-acrylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | (E)-3-(1-phenylmethanesulfonyl-1H-pyrrol-3-yl)-acrylic acid tert-butylester | HCID 66646367 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | (E)-3-(1-phenylmethanesulfonyl-1H-pyrrol-3-yl)-acrylic acid | HCID 66646065 | — |
Reaction Steps
Starting materials: (E)-3-(1-phenylmethanesulfonyl-1H-pyrrol-3-yl)-acrylic acid tert-butylester (compound C2) (1.45 g), CH2Cl2 (80 ml), TFA (8 ml). Reaction conditions: room temperature, 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969401B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-70ae7c92bc2348cfb798b89395a04033 |
| Source note | uspto-grants-2015_03 |