Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Sitagliptin | HCID 4369359 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86647028 | HCID 86647028 | — |
Reaction Steps
Sitagliptin (5 g) and isopropanol (75 mL) are charged into a round-bottom flask and the mixture is heated to about 80° C. for about 30 minutes to obtain a clear dissolution. Oxalic acid (1.54 g) dissolved in water (5 mL) is added and the reaction mixture is refluxed for about 1 hour. The reaction mixture is cooled to about 30° C. and stirred for about 22 hours. The separated solid is filtered, washed with isopropanol (5 mL), and dried under reduced pressure at about 40° C. for about 2.5 hours to afford the title compound. (Yield: 5.8 g; MC: 6.54% w/w; HPLC purity: 99.95%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08969558B2 |
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| Source dataset | uspto-grants-2015_03 |
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| ORD ID | ord-3acafde0a80a4ca4a0c866d82bbe1f75 |
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| Source note | uspto-grants-2015_03 |
|---|