HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 870511Generated: October 30, 2026
Potassium Carbonate → HCID 58072035, compound
https://huagongshe.com/reaction/870511
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1) | HCID 77210 | — |
| Reactant | Benzonitrile, 4-hydroxy-3,5-dimethoxy- | HCID 14381935 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 58072035 | HCID 58072035 | — |
Reaction Steps
6.06 g 3,5 Dimethoxy-4-hydroxy-benzonitrile was dissolved in 20 mL dimethylacetamide, 5.2 g potassium carbonate and 6.7 g N-(2-chloroethyl)morpholine hydrochloride was added and the mixture was stirred at 100° C. for 6 h. The solvent was distilled off and the residue was co-evaporated twice with toluene. The residue was suspended in dichloromethane, filtered and the filtrate was concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08969568B2 |
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| Source dataset | uspto-grants-2015_03 |
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| ORD ID | ord-1eaeacbb9de34bd5a85782af699473a9 |
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| Source note | uspto-grants-2015_03 |
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