HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium borohydride → 1319736-87-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium borohydride | HCID 4148881 | — |
| Reactant | HCID 54291197 | HCID 54291197 | — |
| Solvent | Sodium Chloride | HCID 5234 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1319736-87-2 | HCID 18464561 | — |
Reaction Steps
100 mg Methyl 2-(5-oxopyrrolidine-3-yl)acetate (I.26) was placed in tetrahydrofuran and 30 mg lithium borohydride was added and the mixture stirred at ambient temperature overnight. The suspension was diluted with saturated sodium chloride solution and extracted with ethyl acetate (×3). The water phase was freeze dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969568B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-e0c924d9d353432798a696a1092701aa |
| Source note | uspto-grants-2015_03 |