Phenyl isocyanate → HCID 71621927, compound

Participants

Reaction Steps

A mixture of 5-amino-3-(3-aminophenyl)isothiazole-4-carboxamide (21 mg, 0.090 mmol), N,N-diisopropylethylamine (0.039 mL, 0.23 mmol), and phenyl isocyanate (0.014 mL, 0.13 mmol) in 1.0 mL dioxane was reacted at rt for 1 hour. The precipitant was filtered and rinsed with 30% EtOAc/hexane to give the title compound as a white solid (31 mg, 96%).

Provenance & Evidence