HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2,6,6-Tetramethylpiperidine → HCID 178418821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2,6,6-Tetramethylpiperidine | HCID 13035 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178418821 | HCID 178418821 | — |
Reaction Steps
A solution of LTMP was prepared by reaction of 2,2,6,6-tetramethylpiperidine (0.151 mL, 0.896 mmol) in THF (5.6 mL) and n-butyllithium (0.358 mL, 0.896 mmol) at −30° C. and then at 0° C. for 30 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969586B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-cd8c42b71b59496a9c5b4a16c19569e1 |
| Source note | uspto-grants-2015_03 |