Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Ethylene Oxide | HCID 6354 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Butyl Acrylate | HCID 8846 | — |
| Reactant | Ammonium Persulfate | HCID 62648 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Water | HCID 962 | — |
| Product | Methacrylic Acid | HCID 4093 | — |
| Product | Ethylene Oxide | HCID 6354 | — |
| Product | Styrene-methacrylic acid sodium | HCID 86592924 | — |
Reaction Steps
Into a reaction vessel to which a stirring rod and a thermometer had been set, 683 parts by mass of water, 11 parts by mass of sodium salt of sulfuric acid ester of ethylene oxide adduct of methacrylic acid (“ELEMINOL RS-30,” product of Sanyo Chemical Industries Ltd.), 83 parts by mass of styrene, 83 parts by mass of methacrylic acid, 110 parts by mass of butyl acrylate and 1 part by mss of ammonium persulfate were charged, and then stirred at 400 rpm for 15 min to thereby obtain a white emulsion. The resultant emulsion was heated to a system temperature of 75° C. and was allowed to react for 5 hours. Then, 30 parts by mass of a 1% by mass aqueous ammonium persulfate solution was added thereto, followed by aging at 75° C. for 5 hours, to thereby obtain an aqueous dispersion liquid [fine resin particle dispersion liquid 1] of a vinyl resin (a copolymer of styrene-methacrylic acid-sodium salt of sulfuric acid ester of ethylene oxide adduct of methacrylic acid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08973759B2 |
|---|
| Source dataset | uspto-grants-2015_03 |
|---|
| ORD ID | ord-da04b86e91f14cdfa63bc967e05e2c10 |
|---|
| Source note | uspto-grants-2015_03 |
|---|
