Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 1-(4-ethoxyphenyl)-2-phenylethane-1,2-dione | HCID 1900978 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 58184925 | HCID 58184925 | — |
Reaction Steps
To 0.5 gram of 1-(4-ethoxyphenyl)-2-phenylethane-1,2-dione prepared in Step 1, was add 10 milliliters of concentrated nitric acid and the resulting mixture was heated to 110° C. for 2 hours. The reaction mixture was cooled and poured into 20 milliliters of water. The precipitate was recrystallized from ethanol to give 1-(4-ethoxy-3-nitrophenyl)-2-phenylethane-1,2-dione. The synthesis is summarized by the equation:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08975012B2 |
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| Source dataset | uspto-grants-2015_03 |
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| ORD ID | ord-d7b2ca580c3a454f83defa78930e073a |
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| Source note | uspto-grants-2015_03 |
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