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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 871811Generated: October 31, 2026

Nitric Acid → HCID 58184925, compound

https://huagongshe.com/reaction/871811

Reaction equation

Participants

RoleNameHCIDCharge
ReactantNitric AcidHCID 944—
Reactant1-(4-ethoxyphenyl)-2-phenylethane-1,2-dioneHCID 1900978—
SolventWaterHCID 962—
ProductHCID 58184925HCID 58184925—

Reaction Conditions

Temperature110 °C

Reaction Steps

To 0.5 gram of 1-(4-ethoxyphenyl)-2-phenylethane-1,2-dione prepared in Step 1, was add 10 milliliters of concentrated nitric acid and the resulting mixture was heated to 110° C. for 2 hours. The reaction mixture was cooled and poured into 20 milliliters of water. The precipitate was recrystallized from ethanol to give 1-(4-ethoxy-3-nitrophenyl)-2-phenylethane-1,2-dione. The synthesis is summarized by the equation:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08975012B2
Source datasetuspto-grants-2015_03
ORD IDord-d7b2ca580c3a454f83defa78930e073a
Source noteuspto-grants-2015_03