Gallium(III) nitrate hydrate → Gallium nitrate
Reaction equation
O.[N+:2]([O-:5])([O-:4])=[O:3].[Ga+3:6].[N+:7]([O-:10])([O-:9])=[O:8].[N+:11]([O-:14])([O-:13])=[O:12]>O>[N+:2]([O-:5])([O-:4])=[O:3].[Ga+3:6].[N+:7]([O-:10])([O-:9])=[O:8].[N+:11]([O-:14])([O-:13])=[O:12]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
The stoichiometric amount of gallium-(III)-nitrate hydrate (5.031 g) was dissolved in 80 mL of deionised water to yield gallium nitrate solution. On the other hand, 1.27 g of ammonium metavanadate were dissolved in 100 mL of deionised water at 80° C. The two solutions obtained were mixed under continuous stirring and the pH of the mixture obtained was adjusted to 7 by adding 24% aqueous ammonia solution. A precipitate formed and the suspension obtained was stirred for another half an hour and filtered. The solid obtained was washed several times with deionised water and dried at 120° C. overnight. 2 g of gallium vanadate were obtained and analytically characterised.
Sources & evidence
- ORD record
- ord-1597308fbc9f44ae94f281a4b8999a95
- Source dataset
- uspto-grants-2015_03
- Patent number
- US08975206B2
Reaction notes
Loading…