HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67973724, compound → HCID 90019974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67973724 | HCID 67973724 | — |
| Reactant | 4-nitrophenyl (2S)-1,1,1-trifluoropropan-2-yl carbonate | HCID 68756210 | — |
| Product | HCID 90019974 | HCID 90019974 | — |
Reaction Steps
The title compound is prepared from (S)-5-(1-methanesulfonyl-1,2,3,6-tetrahydro-pyridin-4-yl)-2-methyl-2-piperidin-4-yl-2,3-dihydro-furo[2,3-c]pyridine and carbonic acid 4-nitro-phenyl ester (S)-2,2,2-trifluoro-1-methyl-ethyl ester following a procedure analogous to that described in Example 1. LC (method 3): tR=1.54 min; Mass spectrum (ESI+): m/z=518 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975277B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-1248130929b043048cd078cbca031e13 |
| Source note | uspto-grants-2015_03 |