HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanecarboxylic acid → N-(1-propyl-1H-tetrazol-5-yl)cyclohexane-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanecarboxylic acid | HCID 7413 | — |
| Reactant | 1-propyl-1H-tetrazol-5-amine | HCID 220622 | — |
| Product | N-(1-propyl-1H-tetrazol-5-yl)cyclohexane-carboxamide | HCID 90407822 | 49% |
Reaction Steps
Employing 0.30 g (2.3 mmol) of cyclohexane carboxylic acid and 0.29 mg (2.3 mmol) of 1-propyl-1H-tetrazol-5-amine in the procedure described above and elution with CH2Cl2/MeOH/Et31NT (9.3:0.5:0.2) gave the product in 49% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975288B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-05f62f9da28f40cbbbb6407600d95775 |
| Source note | uspto-grants-2015_03 |