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HRID872482

反应详情

EQUATION

反应方程式

HRID 872482 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NCCOS(C)(=O)=O
HCID22605302

2-[(tert-Butoxycarbonyl)amino]ethyl methanesulfonate

C8H17NO5S

结构：COc1cc([N+](=O)[O-])ccc1-c1ccn[nH]1
HCID67170861

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc([N+](=O)[O-])ccc1-c1ccn(CCN)n1
HCID67172973

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 5-(2-Methoxy-4-nitrophenyl)-1H-pyrazole (1.00 g) and 2-(tert-butoxycarbonylamino)ethyl methanesulfonate (1.42 g) using the method of Example 37(c). Yield 0.24 g (as HCl-salt). 1H-NMR (400 MHz; d6-DMSO): δ 3.32 (t, 2H), 4.02 (s, 3H), 4.47 (t, 2H), 6.94 (d, 1H), 7.88-7.93 (m, 3H), 8.12 (br s, 2H), 8.22 (d, 1H).