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HRID872887

反应详情

EQUATION

反应方程式

HRID 872887 的结构方程式

REACTANTS

反应物

2
结构：CC(Cc1cc(C(=O)O)no1)OC1CCCCO1
HCID67169142

未命名化合物

结构：C[C@H](N)Cn1ccc(-c2ccc(C#N)c(Cl)c2)n1
HCID67170882

4-[1-[(2S)-2-Aminopropyl]-1H-pyrazol-3-yl]-2-chlorobenzonitrile

C13H13ClN4

PRODUCTS

生成物

1
结构：CC(Cc1cc(C(=O)N[C@@H](C)Cn2ccc(-c3ccc(C#N)c(Cl)c3)n2)no1)OC1CCCCO1
HCID70656330

未命名化合物

PROCEDURE

实验过程

The title compound was prepared using the method of Example 34(d) starting from 5-(2-(tetrahydro-2H-pyran-2-yloxy)propyl)isoxazole-3-carboxylic acid (0.392 g, 1.534 mmol) and (S)-4-(1-(2-aminopropyl)-1H-pyrazol-3-yl)-2-chlorobenzonitrile (0.2 g, 0.767 mmol). The product was purified by reverse phase flash chromatography. LC-MS: [M+1]=498.97.

WORKUP

后处理

  1. customThe product was purified by reverse phase flash chromatography